EKSPERIMENT
Iron stone crushed into powders. The
powder was washed with distilled water until clear and then dried in an oven at
a temperature of 70 °C. The dried powder is was separated with a magnetic
separator in other to obtain pure powder Fe2O3.
Then test
the X-ray fluorescence (XRF) to determine the content of the quantitative
elements contained in both the iron ore and which have not been extracted and
test DTA-TGA to determine element mass which is reduced due to temperature
increase.
After that iron powder synthesized by co-precipitation method, in
which the iron powder which has been extracted Fe2O3 was
dissolved in 60 ml HCl 37% M and stirred with a speed of 650 rpm at 70 °C
during 30 minutes. Then FeCl3 solution is formed, later dripped gradually NaOH
solution at temperatures 100 °C until precipitate is formed Fe(OH)3.
After that
precipitate was washed repeatedly with distilled water until pH 7. subsequently
precipitated Fe (OH) 3 produced, then filtered, dried and calcined at a
temperature of 700 ° C, 800 ° C, 860 ° C, 900 ° C with holding time each sample
was 5 hours. The results were characterized with UV-Vis spectrometer to
determine absorbances.
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